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I will however offer the complete reference so that you can track them down. I especially like this paper because of the parallels it draws with other analgesics. They performed acetic acid writhings as well as hot and cold tail flicks. I do have a url.
I was expecting it to sink to the bottom. Hydrobromide you can extract just about any alkaloid using ion exchange chromatography. I think extractions are fine and within the rules.